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table-top NEXAFS system

proXAS

table-top NEXAFS system

  • first integrated NEXAFS spectroscopy solution

  • no need to apply for beamtime

  • chemical state analysis for geology, biology, materials research

  • synchrotron-quality spectra

proXAS is the first system on the market to offer NEXAFS measurements in a laboratory. Fingerprinting for element analysis is now possible in-house with fast and accurate results.

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It combines a highly-reliable laser-based XUV source and a customized spectrometer with an extremely high resolving power of 1900. The energy range 200-1200eV allows for measurements at the K-edge of elements such as C, N, O, Ca, K, Ti.

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Customized versions of proXAS are available. For applications at higher energies, see hiXAS. Please contact us to discuss your application.

Elemental range

Range of elements accessible for table-top NEXAFS measurements

The range of elements accessible to proXAS for NEXAFS measurements includes the K-absorption edges of C, N, O, F, as well as the L-edges of K, Ca, Ti, Cr, Mn, Fe, Co, Ni, Cu.

 

Even diluted samples with analyte concentrations of only 0.2 wt% can be measured.

Downloads

proXAS: table-top NEXAFS system

specifications

Results

NEXAFS sample spectrum goethite hematite

NEXAFS spectrum at the oxygen K-edge of the oxide minerals goethite, hematite, ferrihydrite, and CCa-2 chlorite.

 

(1) measured with the table-top NEXAFS system, measurement time 5min

(2) NEXAFS spectrum recorded at a synchrotron for comparison

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Peak positions deviate by less than 0.06% in energy, underlining the excellent agreement of proXAS measurements with synchrotron data.

NEXAFS sample spectrum carbon K-edge polyimide 1
NEXAFS sample spectrum carbon K-edge polyimide 2

NEXAFS spectrum at the carbon K-edge of PMDA-ODA polyimide.

 

(1) measured with the table-top NEXAFS system, measurement time 2.5min

(2) NEXAFS spectrum recorded at a synchrotron for comparison

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All spectral features, corresponding to transitions of the benzene rings are clearly resolved.

Applications

  • Surface science

  • Chemical state analysis in geochemistry

  • Electronic structure and oxidation state analysis

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